Stepwise Synthesis and Spectral Characteristics of meso-trans-Diphenyldi(1-naphthyl)tetrabenzoporphin and Its Zinc Complex |
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Authors: | Galanin N. E. Kudrik E. V. Shaposhnikov G. P. |
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Affiliation: | (1) Ivanovo State Chemico-technological University, Ivanovo, 153460, Russia |
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Abstract: | A reaction of phthalimide with phenylacetic acid in the presence of zinc oxide furnished 3-oxoisoindolenyl-3'-oxoisoindolinylidene-1,1'-benzylidine which at heating with 1-naphthylacetic acid in the presence of zinc oxide provided zinc meso-trans-diphenyldi(1-naphthyl)tetrabenzoporphin complex. Proceeding from this compound a meso-trans-diphenyldi(1-naphthyl)tetrabenzoporphin was prepared. The spectral characteristics of compounds obtained were studied. |
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