X-Ray spectrometric methods for the determination of plutonium and uranium in their mixed oxide samples |
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Authors: | N C Jayadevan K L Chawla K D Singh Mudher N D Dahale D M Chackraburtty |
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Institution: | (1) Radiochemistry Division, Bhabha Atomic Research Centre, Trombay, 400085 Bombay, India |
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Abstract: | An X-ray fluorescence binary ratio method to measure non-destructively the relative percentage of PuO2 in (U, Pu)O2 samples is described. Calibration lines for pellet and microsphere samples are established and evaluated. Independent X-ray measurement of the major component after dissolution leads to the determination of individual concentrations within ±0.5% rel. of the chemical values. |
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