| 顶空气相色谱-质谱法测定地表水中的1,2-二氯苯 |
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| 引用本文： | 武开业. 顶空气相色谱-质谱法测定地表水中的1,2-二氯苯[J]. 化学分析计量, 2011, 20(3): 67-69 |
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| 作者姓名： | 武开业 |
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| 作者单位： | 陕西省榆林市环境监测总站,榆林,719000 |
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| 摘 要： | 建立了顶空气相色谱-质谱法检测地表水中1,2-二氯苯残留量的方法.选择性离子扫描模式检测,在10～100μg/L范围内1,2-二氯苯浓度与色谱峰面积呈现良好的线生关系,相关系数为0.9996.在20、40μg/L添加水平下,1,2-二氯苯的加标回收率在96.8%～101.7%之间,方法的检出限为5.0μg/L,测定结果...
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| 关 键 词： | 顶空 气相色谱-质谱法 1,2-二氯苯 地表水 |
DETERMINATION OF 1,2-DICHLOROBENZENE IN SURFACE WATER BY HEAD SPACE GAS CHROMATOGRAPHY-MASS SPECTROMETRY |
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| Wu Kaiye. DETERMINATION OF 1,2-DICHLOROBENZENE IN SURFACE WATER BY HEAD SPACE GAS CHROMATOGRAPHY-MASS SPECTROMETRY[J]. Chemical Analysis And Meterage, 2011, 20(3): 67-69 |
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| Authors: | Wu Kaiye |
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| Affiliation: | Wu Kaiye (The Environment Monitoring Center of Yulin in Shannxi Province,Yulin 719000,China) |
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| Abstract: | The method for the determination of 1,2-dichlorobenzene in surface water was developed by head space gas chromatography - mass spectrometry（ HS - GC - MS）. The selective ion scan mode was used to monitor the object. The concentration of 1, 2-dichlorobenzene in surface water had good linearity relationship with the peak area in the range of 10 - 100 μg/L（r = 0.999 6）. The recoveries were 96.8% - 101.7% and the determination limit was 5 μg/L. The RSD of determination results was 3.32% - 3.85% （n = 6 ）. The method has good sensitivity and separating effect, and it can eliminate the interfere from the complex substrate. The method can be applied to determine the residue of the 1,2-dichlorobenzene in the surface water. |
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| Keywords: | head space gas chromatography-mass spectrometry 1 2-dichlorobenzene surface water |
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