| Synthesis of new tetrazene（N-N=N-N）-linked bi（1,2,4-triazole） |
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| 作者姓名： | Sheng Hua Li Si Ping Pang Xiao Tong Li Yong Zhong Yu Xin Qi Zhao |
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| 作者单位： | [1]School of Material Science ＆ Technology, Beijing Institute of Technology, Beijing 10081, China [2]School of Life Science ＆ Technology, Beijing Institute of Technology, Beijing 100081, China |
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| 摘 要： | The reaction of 4-amino-1,2,4-triazole with sodium dichloroisocyanurate (SDCI) afforded new tetrazene(N-N=N-N)-linked bi(1.2,4-triazole) 2a in excellent yield.Increasing the molar ratio of SDCI to 4-amino-1,2,4-triazole,the chlorinated product 1,5,5′- trichloro-4,4′-azo-1,2,4-triazole (2b) was formed.These new compounds have been characterized by MS,~1H NMR,~(13)C NMR,and elemental analysis.
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| 关 键 词： | 三唑 四氮烯 合成方法 药物 |
| 收稿时间： | 25 May 2007 |
| 修稿时间： | 2007-05-25 |
Synthesis of new tetrazene(N-N=N-N)-linked bi(1,2,4-triazole) |
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| Sheng Hua Li Si Ping Pang Xiao Tong Li Yong Zhong Yu Xin Qi Zhao.Synthesis of new tetrazene(N-N=N-N)-linked bi(1,2,4-triazole)[J].Chinese Chemical Letters,2007,18(10):1176-1178. |
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| Authors: | Sheng Hua Li Si Ping Pang Xiao Tong Li Yong Zhong Yu Xin Qi Zhao |
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| Institution: | 1. School of Material Science & Technology, Beijing Institute of Technology, Beijing 10081, China;2. School of Life Science & Technology, Beijing Institute of Technology, Beijing 100081, China |
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| Abstract: | The reaction of 4-amino-1,2,4-triazole with sodium dichloroisocyanurate (SDCI) afforded new tetrazene(N-N=N-N)-linked bi(1,2,4-triazole) 2a in excellent yield. Increasing the molar ratio of SDCI to 4-amino- 1,2,4-triazole, the chlorinated product 1,5,5'-trichloro-4,4'-azo- 1,2,4-triazole (2b) was formed. These new compounds have been characterized by MS, 1H NMR, 13C NMR, and elemental analysis. |
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| Keywords: | Synthesis Triazole Tetrazene |
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