| 水相中无催化剂合成四氢苯并吡喃衍生物 |
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| 引用本文： | 包志坚,纪顺俊,陆军.水相中无催化剂合成四氢苯并吡喃衍生物[J].合成化学,2007,15(5):630-633. |
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| 作者姓名： | 包志坚 纪顺俊 陆军 |
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| 作者单位： | 苏州大学,江苏省有机合成重点实验室,江苏,苏州,215123;苏州大学,化学化工学院,江苏,苏州,215123 |
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| 基金项目： | Supported by the National Natural Science Foundation of China(20472062,20672079)，Supported by a Research Grant from the Innovation Project for graduate students of Jiangsu Province，Supported by the Key Labora-tory of Organic Synthesis of Jiangsu Province(JSK008)，Supported by Nature Science of Jiangsu Province for Higher Ed-ucation(05KJB150116) |
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| 摘 要： | 水相中无催化剂合成了2-氨基-7,7-二甲基-5-氧代-4-芳基-4H-苯并吡喃-3-氰基-5,6,7,8-四氢苯并b]吡喃,其结构经1H NMR,IR和元素分析表征。
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| 关 键 词： | 苯并[b]吡喃 环境友好 无催化剂合成 |
| 文章编号： | 1005-1511（2007）05-0630-04 |
| 收稿时间： | 2007-05-16 |
| 修稿时间： | 2007年5月16日 |
Catalyst-free Synthesis of Tetrahydrobenzo[ b ] pyran Derivatives in Water |
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| BAO Zhi-jian,JI Shun-jun,LU Jun.Catalyst-free Synthesis of Tetrahydrobenzo[ b ] pyran Derivatives in Water[J].Chinese Journal of Synthetic Chemistry,2007,15(5):630-633. |
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| Authors: | BAO Zhi-jian JI Shun-jun LU Jun |
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| Institution: | 1. Key Laboratory of Organic Synthesis of Jiangsu Province; 2. College of Chemistry and Chemical Engineering, Suzhou University, Suzhou 215123, China |
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| Abstract: | Catalyst-free synthesis of 2-amino-7,7-dimethyl-5-oxo-4-aryl-4H-chromene-3-carbonitrile-5,6,7,8-tetrahydrobenzob]pyran(2) in water is described.The structures of 2 were characterized by 1H NMR,IR and elemental analysis. |
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| Keywords: | benzo[b]pyran friendly environment catalyst-free synthesis |
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