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Semi-Micro Preparation and Characterization of Bonded Phase ODS-Silica Prepared from Rice Husk Silica
Authors:Duncan Thorburn Burns  Kanita Tungkananurak  Damrongsak Jadsadapattarakul
Affiliation:(1) School of Chemistry, The Queen’s University of Belfast, BT9 5AG Belfast, Northern Ireland, UK;(2) Department of Chemistry, King Mongkut’s Institute of Technology, 10520 Ladkrabang, Bangkok, Thailand
Abstract:Bonded phase ODS-silica has been prepared using purified silica prepared from rice husk by burning, reflux with sodium hydroxide solution and precipitation as a gel. The gel was spray dried, further purified by washing with concentrated hydrochloric acid then distilled water prior to vacuum drying and silanization and end-capping. The product’s physical and chromatographic properties are reported.
Keywords:: Rice husk   silica   bonded phase   ODS-silica.
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