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A simple sonochemical approach for synthesis and characterization of Zn2SiO4 nanostructures
Institution:1. Prof. C.N.R. Rao Centre for Advanced Materials, Tumkur University, Tumkur 572103, India;2. Department of Physics, B M S Institute of Technology and Management, VTU Affiliated, Bangalore 560064, India;3. Department of Chemistry, University College of Science, Tumkur University, Tumkur 572103, India;1. Laboratory of Physics of Materials and Nanomaterials Applied at Environment (LaPhyMNE), Gabes University, Faculty of Sciences in Gabes, Gabes, Tunisia;2. Al Imam Mohammad Ibn Saud Islamic University (IMSIU), College of Sciences, Department of Physics, Riyadh 11623, Saudi Arabia;1. Research Center of Supercritical Fluid Technology, Tohoku University, 6-6-11, Aramaki Aza Aoba, Aoba-ku, Sendai 980-8579, Japan;2. Graduate School of Environmental Studies, Tohoku University, 6-6-11, Aramaki Aza Aoba, Aoba-ku, Sendai 980-8579, Japan;1. College of Chemical Engineering, Shijiazhuang University, Hebei Province, Shijiazhuang 050035, China;2. Department of Basic Science, Hebei College of Industry and Technology, Hebei Province, Shijiazhuang 050035, China
Abstract:Zn2SiO4 nanoparticles have been successfully prepared via a simple sonochemical method, for the first time. The effect of various parameters including ultrasonic power, ultrasonic irradiation time and different surfactants were investigated to reach optimum condition. The as-prepared nanostructures were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmittance electron microscopy (TEM), Fourier transform infrared (FT-IR) spectra and energy dispersive X-ray microanalysis (EDX). The photocatalytic activity of Zn2SiO4 nano and bulk structures were compared by degradation of anionic dye methyl orange in aqueous solution under UV-light irradiation. Moreover, the cyclic voltammetry analysis of Zn2SiO4 nano and bulk structures were investigated.
Keywords:Nanostructures  Sonochemical method  Electron microscopy  Photocatalytic activity
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