New materials and packing techniques for micro-HPLC packed capillary columns |
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Authors: | A Cappiello P Palma F Mangani |
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Institution: | (1) Istituto di Scienze Chimiche, Università di Urbino, P. Rinascimento 6, 61029 Urbino, Italy |
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Abstract: | Summary Plastic tubing of polyetheretherketone (PEEK) is used for the preparation of HPLC packed capillary columns. The polymer is
rigid but not fragile, has great resistance to chemical and physical agents and comes in standard 1/16″ O.D. These features
can extend the column lifetime and facilitate the overall employment of HPLC capillary columns. Serial connection of short
columns is also possible with no increase in dead volume. A new, rapid and effective packing method has been developed to
be compatible with the characteristics of the material. Several C8 and C18 columns have been prepared and tested and some
applications are shown. |
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Keywords: | Micro-column liquid chromatography Packed capillaries Polyetheretherketone |
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