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Synthesis and Structure of a Bis-calix[4]arene with an o-Xylene Linkage
Authors:Alexandre Mathieu  Zouhair Asfari  Jacques Vicens  Pierre Thuéry  Martine Nierlich
Institution:(1) Laboratoire de Chimie des Interactions Moléculaires, associé, ECPM, au CNRS, 25, rue Becquerel, F-67087, Strasbourg, France;(2) CEA/Saclay, SCM (CNRS URA 331), Bât. 125, 91191 Gif-sur-Yvette, France
Abstract:The reaction of p-tert-butyl calix4]arene 1 withagr,agr'-dibromo-o-xylene in basic conditions leads totwo new compounds. One of them is a bis-calix4]arene, whose crystal structure has been determined.
Keywords:biscalix[4]arenes  crystal structure
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