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Uranium and thorium determination in Brazilian coals by epithermal neutron activation analysis
Authors:L F Bellido  B de C Arezzo
Institution:(1) Instituto de Engenharia Nuclear, Comissão Nacional de Energia Nuclear, C. P. 2186, 20001 Rio de Janeiro, (Brasil);(2) Present address: Comissão Nacional de Energia Nuclear, Rua General Severiano 90, 22294 Rio de Janeiro, Brasil
Abstract:An experimental technique has been developed to determine impurities in coal. Uranium was determined by counting the239Np 106.1 keV gamma-ray with a LEPS detector and thorium by counting the233Pa 311.8 keV gamma-ray with a Ge(Li) detector. Seventeen coal samples were analyzed with an average precision of 3% and a quantitative determination limit of 0.153 mgrg/g for uranium and 0.078 mgrg/g for thorium. The technique allows determinations of up to twenty elements besides U and Th and can be applied in routine analysis.
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