| CdS/有机复合纳米材料的可控合成与表征 |
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| 引用本文： | 李林刚,傅绪成,陈星.CdS/有机复合纳米材料的可控合成与表征[J].化学研究与应用,2011,23(1):51-56. |
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| 作者姓名： | 李林刚 傅绪成 陈星 |
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| 作者单位： | 1. 安徽仿生传感与检测技术省级实验室,安徽,六安,237012;皖西学院材料与化工学院,安徽,六安,237012
2. 安徽仿生传感与检测技术省级实验室,安徽,六安,237012 |
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| 基金项目： | 高等学校安徽省优秀青年人才基金 |
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| 摘 要： | 本文在室温下,以正丁胺为模板剂,二硫化碳为硫源,制得了CdS/有机复合纳米材料.采用XRD、FTIR、SEM、TEM、元素分析以及热重分析(TG)等测试手段对产物进行了表征.实验结果表明产物的结构是CdS(CH3CH2CH2CH2NHCSNHCH2CH2CH2CH3) (CS2).随着正丁胺与二硫化碳的摩尔比、陈化时间...
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| 关 键 词： | 硫化镉 复合纳米材料 合成 表征 |
Controllable synthesis and characterization of CdS/organic nanomaterials |
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| LI Lin-gang,FU Xu-cheng,CHEN Xin.Controllable synthesis and characterization of CdS/organic nanomaterials[J].Chemical Research and Application,2011,23(1):51-56. |
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| Authors: | LI Lin-gang FU Xu-cheng CHEN Xin |
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| Institution: | LI Lin-gang1,2,FU Xu-cheng1,CHEN Xin1(1.Anhui Provincial Laboratory of Biomimetic Sensor and Detecting Technology,Liu'an 237012,China,2.Department of Materials and Chemical engineering,West Anhui University,China) |
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| Abstract: | Taking butylamine and CS2 as template agent and sulfide source,CdS/organic composite nanomaterials were prepared at room temperature.The techiques of XRD,FTIR,SEM,TEM,elemental analyzer and TG were used to characterize the synthesized samples.The results showed that the structure of the products was CdS(CH3CH2CH2CH2NHCSNHCH2CH2CH2CH3)(CS2).As the molar ratio and the aging time of butylamine and CS2 changed,the morphology of the product was also changed from nano-particles,nano-lines to nanobelts. |
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| Keywords: | cadmium sulfide composite nanomaterials synthesis character |
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