| 有机电致发光材料噁二唑衍生物的合成 |
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| 引用本文： | 孙一峰,宋化灿,李卫明,许遵乐. 有机电致发光材料噁二唑衍生物的合成[J]. 有机化学, 2003, 23(11): 1286-1290 |
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| 作者姓名： | 孙一峰 宋化灿 李卫明 许遵乐 |
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| 作者单位： | 中山大学化学与化学工程学院,广州,510275 |
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| 基金项目： | 广州市科委基金 (No .2 0 0 1 J 0 1 5 0 1 )资助项目 |
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| 摘 要： | 由酰氯与各种酰肼反应得到中间体4，进而用三氯氧磷脱水闭环，合成了一系 列1，3，4-噁二唑衍生物5，用~1H NMR，IR，MS和元素分析对其结构进行了确证。
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| 关 键 词： | 电致发光 恶二唑 P 酰氯 酰肼 质子磁共振谱法 红外分光光度法 质谱法 元素分析 结构表征 香豆素 |
| 修稿时间： | 2002-11-04 |
Synthesis of 1,3,4-Oxadiazole Derivatives for Organic Electro- transporting Electroluminesent Materials |
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| SUN,Yi-Feng SONG,Hua-Can LI,Wei-Ming XU,Zun-Le. Synthesis of 1,3,4-Oxadiazole Derivatives for Organic Electro- transporting Electroluminesent Materials[J]. Chinese Journal of Organic Chemistry, 2003, 23(11): 1286-1290 |
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| Authors: | SUN Yi-Feng SONG Hua-Can LI Wei-Ming XU Zun-Le |
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| Affiliation: | School of Chemistry and Chemical Engineering, Zhongshan University |
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| Abstract: | Oxadiazole derivatives (5) were prepared from hydrazide (3), which were converted with acyl~chlo~ride in pyridine into N-substituted hydriazide (4), followed by treatment with phosphorus oxychloride. The newly synthesized compounds were characterized by 1H NMR, IR, MS and elemental analyses. These compounds represent potential organic electro-transporting electroluminesent (EL) materials. |
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| Keywords: | 1 3 4-oxadiazole coumarin electron transport material electroluminesent (EL) synthesis |
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