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Retention behavior and solvent optimization of organochlorine pesticides in solid-phase extraction |
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| Authors: | E. B. Asafu-Adjaye P. W. Kohler S. Y. Su |
| Affiliation: | (1) Department of Chemistry, Virginia Commonwealth University, 23284 Richmond, VA, USA;(2) Present address: Division of Solid and Hazardous Waste Management, Commonwealth of Virginia, 23219 Richmond, VA, USA |
| Abstract: | Summary Plots of capacity factor and retention time vs. elution solvent composition were proved to be useful to interpret the retention behavior of Kepone and its metabolites in a reversed-phase solid-phase extraction and to optimize the elution solvent. The percent recovery of Kepone was largely improved when the solvent was optimized. The standard deviations of the results of extractions were also improved upon the optimization of the solvent. |
| Keywords: | Solid-phase extraction Solvent optimization Organochlorine pesticides Capacity factor Sample preparation |
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