| 二(三)丁基锡烯基(炔基)膦酸酯的合成与表征 |
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| 引用本文： | 尹汉东,马春林,张如芬. 二(三)丁基锡烯基(炔基)膦酸酯的合成与表征[J]. 有机化学, 2000, 20(1): 108-111 |
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| 作者姓名： | 尹汉东 马春林 张如芬 |
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| 作者单位： | 聊城师范学院化学系,聊城252059 |
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| 基金项目： | 山东省自然科学基金资助课题 |
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| 摘 要： | 合成了12个新的二(三)丁基锡烯基(炔基)膦酸酯[(n-C4H9)nSn]n-1O2P(0)R，并用元素分析，红外光谱，核磁共振氢谱和TG-DTA对其组成和结构进行了表征，初步生物活性测试表明，有些化合物具有较强的杀螨和杀菌活性。
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| 关 键 词： | 膦酸酯类 有机锡化合物 杀虫剂 生物活性 元素分析 红外分光光度法 核磁共振谱法 差热分析 热重量分析 结构表征 |
| 修稿时间： | 1998-11-20 |
Synthesis and characterization of Di - (or Tri) butyltin alkenyl (or alkynyl) phosphates |
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| Yin Han-Dong,Ma Chun-Lin,Zhang Ru-Fen. Synthesis and characterization of Di - (or Tri) butyltin alkenyl (or alkynyl) phosphates[J]. Chinese Journal of Organic Chemistry, 2000, 20(1): 108-111 |
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| Authors: | Yin Han-Dong Ma Chun-Lin Zhang Ru-Fen |
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| Affiliation: | Yin Han- Dong,Ma Chun- Lin,Zhang Ru- Fen(Department of chemistry, Liaocheng Teachers college, 252059 Liaocheng) |
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| Abstract: | Twelve new di - (or tri) butyltin alkenyl (or alkynyl) phosphates of general formular [(n - C4H9)nSn]n-1O2P(O) R (n=2,3; R= -CH = CClPh, - C ≡ CC5H11-n, - C ≡ CC6H13-n, - C≡CPh, C≡CCH2OMe, C≡CCH2OEt) were synthesized and characterized by elemental analysis, IR, ^1H NMR spectra and TG-DTA. The bioassay of some compounds showed that they had better miticidal activity and fungicidal activity. |
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| Keywords: | butyltin alkenyl (or alkynyl) phosphate bioassay |
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