Spectroscopic Studies and Structure of 4-(3-Benzoylthioureido)benzoic Acid |
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| Authors: | Fatma Aydın Hüseyin Ünver Doğan Aykaç Nazan Ocak İskeleli |
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| Affiliation: | 1.Faculty of Science and Arts, Department of Chemistry,?anakkale Onsekiz Mart University,?anakkale,Turkey;2.Faculty of Science, Department of Physics,Ankara University,Ankara,Turkey;3.Department of Science Education,Ondokuz May?s University,Samsun,Turkey |
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| Abstract: | Abstract 4-(3-Benzoylthioureido)benzoic acid has been synthesized from the reaction of 4-aminobenzoic acid with benzoyl isothiocyanate. The title compound has been characterized by elemental analysis, MS, FT-IR, 1H-NMR, 13C-NMR and UV–Visible techniques. The structure of the compound has also been examined crystallographically. The title compound crystallizes in the triclinic space group P-1 with a = 3.969(1), b = 13.039(1), c = 13.504(1) ?, α = 96.50(1)°, β = 92.25(1)°, γ = 94.94(1), V = 691.0(1) ?3 and D x = 1.444 g cm−3, respectively. The crystal structure has been solved by direct methods and refined by full-matrix least squares and found R 1 = 0.031 and wR 2 = 0.081 for 2909 observed reflections [I > 2σ(I)]. |
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