等离子体原子荧光光谱法测定碳酸锂中钠、钾、钙、镁、铜、铁、钴、镍、锰、锌、镉 |
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引用本文: | 陈先安.等离子体原子荧光光谱法测定碳酸锂中钠、钾、钙、镁、铜、铁、钴、镍、锰、锌、镉[J].分析化学,1989(11). |
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作者姓名: | 陈先安 |
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作者单位: | 北京有色金属研究总院 北京,100088 |
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摘 要: | 建立了用ICP-AFS同时测定碳酸锂中11种微量金属杂质元素的方法。加入甲烷可改善检出限,方法简便,样品分析结果与AAS法结果一致。
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关 键 词: | JCP-AFS 钠 钾 钙 镁 铜 铁 钴 镍 锰 锌 镉 碳酸锂 |
DETERMINATION OF Na,K,Ca,Mg,Cu,Fe,Co,Ni,Mn,Zn AND Cd IN LITHIUM CARBONATE BY ICP-ATOMIC FLUORESCENCE SPECTROMETRY |
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Institution: | Beijing General Research Institute for Non-Ferrous Metals |
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Abstract: | A simultaneous determination procedure for multielements of micro amounts of Na, K, Ca, Mg, Cu, Fe, Co, Ni, Mn, Zn and Cd in lithium carbonate by ICP-AFS has been presented. The standard addition method can be used to eliminate the matrix and interelement interferences. The detection limits of some elements to be determined can be improved with a concentric flow pneumatic nebulizer and further using methane as reductant. |
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Keywords: | ICP-AFS Sodium Potassium Calcium Magnesium Copper Iron Cobalt Nickel Manganese Zinc Cadmium Lithium carbonate |
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