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1H and 13C spectral assignment of symmetrical bis[(4-aminosubstituted)quinolinium] derivatives
Authors:Campos Joaquín M  Sánchez-Martín Rosario M  Cruz-López Olga  Conejo-García Ana  Gallo Miguel A  Espinosa Antonio
Affiliation:Departamento de Química Farmacéutica y Orgánica, Facultad de Farmacia, Universidad de Granada, C/Campus de Cartuja, s/n. 18071 Granada, Spain.
Abstract:1H and 13C NMR spectroscopic data of both the quinolinium ring and the spacers for 32 symmetrical bisquinolinium compounds were assigned by a combination of one- and two-dimensional experiments (DEPT, HMBC, HMQC). The compounds have electron-releasing groups at position 4 of the quinolinium ring, with several arylalkyl linkers such as the 3,3'-, 4,4'-bis(methylene)biphenyl and 4,4'-bis(methylene)bibenzyl moieties.
Keywords:NMR  1H NMR  13C NMR  2D NMR  HMQC  HMBC  arylalkyl linkers  bisquinolinium salts
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