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1H and 13C NMR spectral assignments of pyridinium salts linked to a N‐9 or N‐3 adenine moiety |
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| Authors: | Belén Rubio‐Ruiz Ana Conejo‐García Miguel A. Gallo Antonio Espinosa Antonio Entrena |
| Affiliation: | Departamento de Química Farmacéutica y Orgánica, Facultad de Farmacia, Universidad de Granada, , 18071 Granada, Spain |
| Abstract: | 1H and 13 C NMR spectral data of 13 new compounds containing a 4‐(dimethylamino)‐ or 4‐(pyrrolidin‐1‐yl)pyridinium moiety linked to the N‐9 or N‐3 nitrogen atom of an adenine moiety were assigned. 1D and 2D NMR experiments (DEPT, HSQC and HMBC) allowed the unequivocal identification of N‐9 and N‐3 isomers. Copyright © 2012 John Wiley & Sons, Ltd. |
| Keywords: | NMR 1H and 13C 1D NMR 1H‐13C 2D NMR (HSQC, HMBC) choline kinase inhibitors antiproliferative compounds |