| μ-氧-双[三(对氟苄基)锡]的合成、表征及晶体结构 |
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| 引用本文： | 尹汉东,洪敏,王传华. μ-氧-双[三(对氟苄基)锡]的合成、表征及晶体结构[J]. 无机化学学报, 2005, 21(5): 713-715 |
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| 作者姓名： | 尹汉东 洪敏 王传华 |
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| 作者单位： | 聊城大学化学系,聊城,252059 |
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| 基金项目： | 国家自然科学基金(No.20271025)，山东省自然科学基金(No.L2003B01)资助课题。 |
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| 摘 要： | The μ-oxygen-bis[tri(p-fluorobenzyl)tin] was synthesized. The structure were characterized by elementary analysis, IR and 1H NMR and the crystal structure were determined by X-ray single crystal diffraction. The crystal of the title compound belongs to rhombohedral with space group R, a=1.346 4(4), b=1.346 4(4), c=1.772 9(7) nm, α=90°, β=90°, γ=120°, Z=3, V=2.783 2(15) nm3, Dc=1.625 g·cm-3, μ(Mo Kα)=1.408 mm-1, S=1.088, F(000)=1 350, R1=0.027 5, wR2=0.065 9. In compound, the tin atom has a distorted tetrahedral coordination configuration. CCDC: 257079.
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| 关 键 词： | μ-氧-双[三(对氟苄基)锡]； 合成； 晶体结构 |
| 文章编号： | 1001-4861(2005)05-0713-03 |
| 收稿时间： | 2004-09-20 |
| 修稿时间： | 2004-09-20 |
Synthesis,Characterization and Crystal Structures of the μ-Oxygen-Bis[Tri(p-Fluorobenzyl)tin] |
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| YIN Han-Don,HONG Min and WANG Chuan-Hua. Synthesis,Characterization and Crystal Structures of the μ-Oxygen-Bis[Tri(p-Fluorobenzyl)tin][J]. Chinese Journal of Inorganic Chemistry, 2005, 21(5): 713-715 |
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| Authors: | YIN Han-Don HONG Min WANG Chuan-Hua |
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| Affiliation: | Department of Chemistry, Liaocheng University, Liaocheng 252059,Department of Chemistry, Liaocheng University, Liaocheng 252059 and Department of Chemistry, Liaocheng University, Liaocheng 252059 |
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