| Synthesis of novel chiral stationary phases for high-performance liquid chromatography |
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| 作者姓名： | Xu Lin Tan Shi Cong Hou Qing Hua Bian Min Wang |
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| 作者单位： | Xu Lin Tan，Shi Cong Hou，Qing Hua Bian，Min Wang* College of Science，China Agricultural University，Beijing 100094，China |
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| 摘 要： | Three novel chiral selectors 4a-c were synthesized from(S)-amino acids and(R)-1-phenyl-2-(4-methylphenyl)ethylamine.4a-cwere connected to 3-aminopropylsilanized silica gel to be used as the chiral stationary phase for HPLC.Five amino acid derivativesand two pyrethroid insecticides were fairly resolved on these three new chiral stationary phases under normal phase condition.
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| 关 键 词： | 手性固定相 合成 高效液相色谱法 氨基酸衍生物 对映体 |
| 收稿时间： | 2006-11-29 |
Synthesis of novel chiral stationary phases for high-performance liquid chromatography |
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| Xu Lin Tan Shi Cong Hou Qing Hua Bian Min Wang.Synthesis of novel chiral stationary phases for high-performance liquid chromatography[J].Chinese Chemical Letters,2007,18(4):461-464. |
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| Authors: | Xu Lin Tan Shi Cong Hou Qing Hua Bian Min Wang |
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| Institution: | College of Science, China Agricultural University, Beijing 100094, China |
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| Abstract: | Three novel chiral selectors 4a-c were synthesized from(S)-amino acids and(R)-1-phenyl-2-(4-methylphenyl)ethylamine.4a-c were connected to 3-aminopropylsilanized silica gel to be used as the chiral stationary phase for HPLC.Five amino acid derivatives and two pyrethroid insecticides were fairly resolved on these three new chiral stationary phases under normal phase condition. |
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| Keywords: | Enantioseparation Chiral stationary phase Amino acid derivatives Pyrethroid insecticides |
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