Mechanism and kinetics of synthesizing dibutoxymethane by phase transfer catalysis |
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| Authors: | Maw-Ling Wang and Shahng-Wern Chang |
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| Affiliation: | (1) Department of Chemical Engineering, Tsing Hua University, 30043 Hsinchu, Taiwan, ROC |
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| Abstract: | The synthesis of CH2(OC4H9)2 by phase transfer catalysis (PTC) has been studied in C6H5Cl/KOH solution. A pseudo-first-order rate law was applied for describing the reaction at a rather high [KOH]w. The reaction system was limited by the reaction equilibrium in the aqueous phase at low [KOH]w and the reaction in the organic phase at high [KOH]w. |
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