| 银纳米微球和银纳米棒自组装膜的制备及SERS研究 |
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| 引用本文： | 李莉,鲁峰,杨武. 银纳米微球和银纳米棒自组装膜的制备及SERS研究[J]. 影像科学与光化学, 2016, 34(4): 329-335. DOI: 10.7517/j.issn.1674-0475.2016.04.329 |
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| 作者姓名： | 李莉 鲁峰 杨武 |
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| 作者单位： | 1. 甘肃有色冶金职业技术学院, 甘肃 金昌 737100;2. 西北师范大学 化学化工学院 生态环境相关高分子材料教育部重点实验室, 甘肃 兰州 730070 |
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| 基金项目： | 国家自然科学基金(20873101)，教育部教育管理信息中心2015年岗位模型课题研究项目(JYB-EMIC-15021) |
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| 摘 要： | 采用硼氢化钠还原硝酸银,用振荡器在不同转速下振荡得到单分散的银纳米微球和银纳米棒,再将银纳米微球及银纳米棒自组装于被3-氨丙基-三甲氧基硅烷(APTMS)修饰的玻璃基片上,制得了具有表面增强拉曼(SERS)活性的基底,分别以罗丹明6G(R6G)和罗丹明B(RB)为探针分子对这两种基底进行SERS活性检测,结果发现这两种基底均为较理想的SERS衬底。
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| 关 键 词： | 银纳米微球 银纳米棒 自组装 SERS |
| 收稿时间： | 2015-12-04 |
Preparation of Self-assembled Films of Silver Nanoparticles and Silver Nanorods for SERS Research |
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| LI Li,LU Feng,YANG Wu. Preparation of Self-assembled Films of Silver Nanoparticles and Silver Nanorods for SERS Research[J]. Imaging Science and Photochemistry, 2016, 34(4): 329-335. DOI: 10.7517/j.issn.1674-0475.2016.04.329 |
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| Authors: | LI Li LU Feng YANG Wu |
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| Affiliation: | 1. Gansu Vocational & Technical College of Nonferrous Metallurgy, Jinchang 737100, Gansu,P.R.China;2. Key Lab of Eco-Environmental Related Polymer Materials of MOE, College of Chemistry & Chemical Engineering, Northwest Normal University, Lanzhou 730070, Gansu, P.R.China |
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| Abstract: | With different rotational speed of agitator, the silver nanoparticles and silver nanorods were obtained by the reduction of sodium borohydride. Then the silver nanoparticles and nanorods were self-assembed on a glass plate modified by the silane reagent 3-aminopropyltrimethoxysilane (APTMS). The glass plate was prepared as surface-enhanced Raman scattering (SERS) active basement, with Rhodamine 6G (R6G) and Rhodamine B (RB) molecular probes for the detection of the two substrates' SERS activities. The results showed that the two substrates are ideal SERS substrates. |
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| Keywords: | silver nanoparticles silver nanorods self-assembled SERS |
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