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The use of vacuum in thin-layer chromatography with a forced flow of the mobile phase on plates with covered polymer layer
Authors:V. G. Berezkin  V. V. Buzaev
Affiliation:(1) A. V Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, 29 Leninsky prosp., 117912 Moscow, Russian Federation
Abstract:A new version of TLC with a forced flow of the mobile phase has been suggested. The variant involves the use of a TLC plate, the sorption layer on which is covered with a polymer film, and evacuation as an additional driving force for the mobile phase. The advantages of the new method were analyzed; the velocity coefficient of the movement of the mobile phase front was found to be linearly dependent on the rarefaction at the end of the plate.Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 5, pp. 1143–1146, May, 1996.
Keywords:thin-layer chromatography  mobile phase  forced flow  vacuum
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