Coulometric method for the microdetermination of active hydrogen in organic compounds |
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| Authors: | G. F. Anisimova V. A. Klimova |
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| Affiliation: | (1) N. D. Zelinskii Institute of Organic Chemistry, Academy of Sciences of the USSR, USSR |
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| Abstract: | Conclusions An automatic, simple, and rapid coulometric method is proposed for the microdetermination of active hydrogen in organic compounds. The method is based on the reaction of active hydrogen with LiAlH4, combustion of the hydrogen formed to water, and measurement of the amount of electricity expended in its electrolysis.Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 3, pp. 581–583, March, 1972. |
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