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Synthesis,Characterization, and Crystal Structure of a New Coordination Polymer of Lead(II) Containing 2,6‐Pyridinedicarboxylic Acid
Authors:Masoud Rafizadeh  Vahid Amani  Bernhard Neumüller
Abstract:The reaction of solution 2,6‐pyridinedicarboxylic acid ( 1 ) and 2,2′‐Bipyridine with Pb(NO3)2 led to the coordination polymer Pb(pydc)]n ( 2 ) (pydcH2 is 2,6‐pyridinedicarboxylic acid). This complex was characterized by elemental analysis, IR spectroscopy and single‐crystal structure of 2 . Crystal data for 2 at ?80 °C: monoclinic, space group P21/n, a = 977.2(1), b = 554.0(1), c = 1425.3(2) pm, β = 104.75(1)°, Z = 4, R1= 0.0261. The units Pb(pydc)] form infinite chains along 010].
Keywords:Lead(II)  2  6‐Pyridinedicarboxylic acid  Crystal structure
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