One-pot solid phase synthesis of (E)-nitroalkenes |
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Authors: | Lalthazuala Rokhum Ghanashyam Bez |
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Affiliation: | Department of Chemistry, North Eastern Hill University, Shillong 793022, India |
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Abstract: | An efficient one-pot protocol for the synthesis of (E)-nitroalkenes by reaction of aldehydes and nitroalkanes in the presence of polymer-bound triphenylphosphine, iodine and imidazole is described. Although the reaction works with similar efficiency with triphenylphosphine and its polymer-bound version, easy removal of the unwanted polymer-bound triphenylphosphine oxide and its recovery as triphenylphosphine provide the edge for practical application of the method. |
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Keywords: | (E)-Nitroalkenes Polymer-bound triphenylphosphine Iodine Imidazole Solid phase synthesis |
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