Measurement of the thermal capacity of solids by DSC |
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Authors: | G K Demensky O A Teplov |
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Institution: | (1) Baykov Institute of Metallurgy, Academy of Sciences of the U.S.S.R., USSR |
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Abstract: | The methods for determining the thermal capacity of solids using a SETARAM DSC-III calorimeter have been studied. Two methods can be employed: periodic heating and continuous heating. The method using periodic heating is characterized by an accuracy of 0.6%,'while the method with continuous heating has an accuracy of 5%. Thermal capacity measurements on corundum, copper oxide and magnetite are reported.
Zusammenfassung Methoden zur Bestimmung der Wärmekapazität von Festkörpern wurden mittels des Kalorimeters SETARAM DSC-III untersucht. Zwei Methoden können angewandt werden, nämlich periodisches und kontinuierliches Aufheizen. Bei periodischem Heizen beträgt die Genauigkeit 0,6%, bei kontinuierlichem 5%. Über Messungen der Wärmekapazität von Korund, Kupferoxid und Magnetit wird berichtet.
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