| An Expedient Method for the Synthesis of Thiosemicarbazones under Microwave Irradiation in Solvent-free Medium |
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| 引用本文： | 李建平 郑鹏志 朱俊歌 刘锐杰 渠桂荣. An Expedient Method for the Synthesis of Thiosemicarbazones under Microwave Irradiation in Solvent-free Medium[J]. 中国化学, 2006, 24(12): 1773-1776. DOI: 10.1002/cjoc.200690331 |
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| 作者姓名： | 李建平 郑鹏志 朱俊歌 刘锐杰 渠桂荣 |
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| 作者单位： | College of Chemistry and Environmental Science, Henan Normal University, The Key Laboratory of Environmental Pollution Control of Henan Province, Xinxiang, Henan 453007, China |
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| 基金项目： | Project supported by the National Natural Science Foundation of China （No. 20372018）. |
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| 摘 要： | A simple,efficient and eco-friendly method for the synthesis of thiosemicarbazones from thiosemicarbazidesand aldehyde under microwave irradiation has been reported,and no solvent and catalyst were used.And the tech-nique of microwave irradiation coupled with solvent-free condition proved to be a quite valuable method in the or-ganic synthesis.
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| 关 键 词： | 缩氨基硫脲 氨基硫脲 乙醛 微波照射 自由溶剂 |
| 收稿时间： | 2006-03-17 |
| 修稿时间： | 2006-03-172006-07-10 |
An Expedient Method for the Synthesis of Thiosemicarbazones under Microwave Irradiation in Solvent-free Medium |
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| LI Jian-Ping, ZHENG Peng-Zhi, ZHU Jun-Ge, LIU Rui-Jie, QU Gui-Rong. An Expedient Method for the Synthesis of Thiosemicarbazones under Microwave Irradiation in Solvent-free Medium[J]. Chinese Journal of Chemistry, 2006, 24(12): 1773-1776. DOI: 10.1002/cjoc.200690331 |
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| Authors: | LI Jian-Ping ZHENG Peng-Zhi ZHU Jun-Ge LIU Rui-Jie QU Gui-Rong |
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| Affiliation: | College of Chemistry and Environmental Science, Henan Normal University, The Key Laboratory of Environmental Pollution Control of Henan Province, Xinxiang, Henan 453007, China |
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| Abstract: | A simple, efficient and eco-friendly method for the synthesis of thiosemicarbazones from thiosemicarbazides and aldehyde under microwave irradiation has been reported, and no solvent and catalyst were used. And the technique of microwave irradiation coupled with solvent-free condition proved to be a quite valuable method in the organic synthesis. |
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| Keywords: | thiosemicarbazone thiosemicarbazide aldehyde microwave solvent-free |
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