Effect of quartz substrate on adsorption and texture properties of titanium-containing silica membranes |
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Authors: | A. I. Ivanets T. F. Kuznetsova V. G. Prozorovich S. I. Eremenko |
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Affiliation: | 1631. Institute of General and Inorganic Chemistry, National Academy of Sciences of Belarus, Minsk, Belarus
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Abstract: | Sol-gel method with joint hydrolysis of silicon and titanium alkoxides were used to synthesize titanium-containing silica membranes on a macroporous quartz substrate. Isotherms of low-temperature adsorption-desorption of nitrogen by the samples obtained were measured. Characteristic features inherent in mesoporous samples were found in the isotherms. A change in the adsorption properties of the membranes was observed upon a preliminary treatment of the substrate with a mixture of hydrogen peroxide and concentrated sulfuric acid. |
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