Two-dimensional and variable temperature 31P solid-state NMR studies of single crystals containing symmetrical/unsymmetrical bis[6-O,6-O'-(1,2:3,4-diisopropylidene-alpha-D- galactopyranosyl)thiophosphoryl] dichalcogenides |
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| Authors: | Potrzebowski M J Helinski J Ciesielski W |
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| Institution: | Department of Structural Studies, Centre of Molecular and Macromolecular Studies, Polish Academy of Sciences, Sienkiewicza 112, PL-90-363 ?ód?, Poland. marekpot@bilbo.cbmm.lodz.pl |
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| Abstract: | The organisation and phase transition of single crystals containing three isostructural bis6-O,6-O'-(1,2:3,4-diisopropylidene-alpha- D-galactopyranosyl)thiophosphoryl] dichalcogenide derivatives: disulfide 1, diselenide 2 and mixed seleno-sulfide 3, was deduced upon 1D, 2D and variable temperature 31P NMR experiments. |
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