Total synthesis of clathculins A and B |
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| Authors: | Hoye Rebecca C Anderson Gretchen L Brown Susan G Schultz Erica E |
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| Affiliation: | Department of Chemistry, Macalester College, 1600 Grand Avenue, Saint Paul, Minnesota 55105, United States. hoye@macalester.edu |
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| Abstract: | Clathculins A and B represent a new class of vic-diamine alkaloids containing a PA2 unit as the basic structure. We report the first total syntheses of 1 and 2, which confirm the assigned structure of each. Dependence of their NMR spectroscopic behavior as a function of protonation state has been observed. |
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