A novel possibility to clarify the role of bromide in bromate oscillators |
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Authors: | E Krös and M Varga |
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Institution: | (1) Institute of Inorganic and Analytical Chemistry, L. Eötvös University, Box 123, H-1443 Budapest, Hungary |
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Abstract: | Bromocomplex forming metal ions (Tl3+, Hg2+) alter considerably the parameters of chemical oscillations in bromate oscillators. Even at 10–5 M metal ion concentration the period of the oscillation is doubled or tripled; at 10–4 M the oscillation is quenched. At high ( 10–2 M) Tl3+ concentration, high frequency, strongly damped oscillations occur although Br–]eq is below 10–10 M. By the addition of Tl3+ we could determine the amount of Br– formed in a single autocatalytic step, which we found to be about 10–4 M.
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![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![rcy](/content/qh19t408400367q6/xxlarge1088.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) . ![Dcy](/content/qh19t408400367q6/xxlarge1044.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![zhcy](/content/qh19t408400367q6/xxlarge1078.gif) ![pcy](/content/qh19t408400367q6/xxlarge1087.gif) ![rcy](/content/qh19t408400367q6/xxlarge1088.gif) ![kcy](/content/qh19t408400367q6/xxlarge1082.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![tscy](/content/qh19t408400367q6/xxlarge1094.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![rcy](/content/qh19t408400367q6/xxlarge1088.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![tscy](/content/qh19t408400367q6/xxlarge1094.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![yacy](/content/qh19t408400367q6/xxlarge1103.gif) ![mcy](/content/qh19t408400367q6/xxlarge1084.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![chcy](/content/qh19t408400367q6/xxlarge1095.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![kcy](/content/qh19t408400367q6/xxlarge1082.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) 10–5 M ![pcy](/content/qh19t408400367q6/xxlarge1087.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![rcy](/content/qh19t408400367q6/xxlarge1088.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![kcy](/content/qh19t408400367q6/xxlarge1082.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![bcy](/content/qh19t408400367q6/xxlarge1073.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![bcy](/content/qh19t408400367q6/xxlarge1073.gif) ![ucy](/content/qh19t408400367q6/xxlarge1091.gif) ![dcy](/content/qh19t408400367q6/xxlarge1076.gif) ![vcy](/content/qh19t408400367q6/xxlarge1074.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) , ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![bcy](/content/qh19t408400367q6/xxlarge1073.gif) ![ucy](/content/qh19t408400367q6/xxlarge1091.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![rcy](/content/qh19t408400367q6/xxlarge1088.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ; ![pcy](/content/qh19t408400367q6/xxlarge1087.gif) ![rcy](/content/qh19t408400367q6/xxlarge1088.gif) 10–4 M ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![tscy](/content/qh19t408400367q6/xxlarge1094.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![yacy](/content/qh19t408400367q6/xxlarge1103.gif) ![tscy](/content/qh19t408400367q6/xxlarge1094.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![gcy](/content/qh19t408400367q6/xxlarge1075.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) . ![Pcy](/content/qh19t408400367q6/xxlarge1055.gif) ![rcy](/content/qh19t408400367q6/xxlarge1088.gif) ![vcy](/content/qh19t408400367q6/xxlarge1074.gif) ![ycy](/content/qh19t408400367q6/xxlarge1099.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![kcy](/content/qh19t408400367q6/xxlarge1082.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![kcy](/content/qh19t408400367q6/xxlarge1082.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![tscy](/content/qh19t408400367q6/xxlarge1094.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![rcy](/content/qh19t408400367q6/xxlarge1088.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![yacy](/content/qh19t408400367q6/xxlarge1103.gif) Tl3+ ( 10–2 M) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![bcy](/content/qh19t408400367q6/xxlarge1073.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![yucy](/content/qh19t408400367q6/xxlarge1102.gif) ![dcy](/content/qh19t408400367q6/xxlarge1076.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![tscy](/content/qh19t408400367q6/xxlarge1094.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![yacy](/content/qh19t408400367q6/xxlarge1103.gif) ![tscy](/content/qh19t408400367q6/xxlarge1094.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![vcy](/content/qh19t408400367q6/xxlarge1074.gif) ![ycy](/content/qh19t408400367q6/xxlarge1099.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![kcy](/content/qh19t408400367q6/xxlarge1082.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![chcy](/content/qh19t408400367q6/xxlarge1095.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) 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![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![ucy](/content/qh19t408400367q6/xxlarge1091.gif) ![dcy](/content/qh19t408400367q6/xxlarge1076.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) , ![khcy](/content/qh19t408400367q6/xxlarge1093.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) Br–]eq ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![zhcy](/content/qh19t408400367q6/xxlarge1078.gif) 10–10 M. ![Dcy](/content/qh19t408400367q6/xxlarge1044.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![bcy](/content/qh19t408400367q6/xxlarge1073.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![vcy](/content/qh19t408400367q6/xxlarge1074.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) Tl3+ ![ucy](/content/qh19t408400367q6/xxlarge1091.gif) ![dcy](/content/qh19t408400367q6/xxlarge1076.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![pcy](/content/qh19t408400367q6/xxlarge1087.gif) ![rcy](/content/qh19t408400367q6/xxlarge1088.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![dcy](/content/qh19t408400367q6/xxlarge1076.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![kcy](/content/qh19t408400367q6/xxlarge1082.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![chcy](/content/qh19t408400367q6/xxlarge1095.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![vcy](/content/qh19t408400367q6/xxlarge1074.gif) Br–, ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![bcy](/content/qh19t408400367q6/xxlarge1073.gif) ![rcy](/content/qh19t408400367q6/xxlarge1088.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![zcy](/content/qh19t408400367q6/xxlarge1079.gif) ![ucy](/content/qh19t408400367q6/xxlarge1091.gif) ![yucy](/content/qh19t408400367q6/xxlarge1102.gif) ![shchcy](/content/qh19t408400367q6/xxlarge1097.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![gcy](/content/qh19t408400367q6/xxlarge1075.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![dcy](/content/qh19t408400367q6/xxlarge1076.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![vcy](/content/qh19t408400367q6/xxlarge1074.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![vcy](/content/qh19t408400367q6/xxlarge1074.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![kcy](/content/qh19t408400367q6/xxlarge1082.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![icy](/content/qh19t408400367q6/xxlarge1080.gif) ![chcy](/content/qh19t408400367q6/xxlarge1095.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![kcy](/content/qh19t408400367q6/xxlarge1082.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![ucy](/content/qh19t408400367q6/xxlarge1091.gif) ![pcy](/content/qh19t408400367q6/xxlarge1087.gif) ![iecy](/content/qh19t408400367q6/xxlarge1077.gif) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) , ![kcy](/content/qh19t408400367q6/xxlarge1082.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![tcy](/content/qh19t408400367q6/xxlarge1090.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![rcy](/content/qh19t408400367q6/xxlarge1088.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![kcy](/content/qh19t408400367q6/xxlarge1082.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![zcy](/content/qh19t408400367q6/xxlarge1079.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![lcy](/content/qh19t408400367q6/xxlarge1083.gif) ![ocy](/content/qh19t408400367q6/xxlarge1086.gif) ![scy](/content/qh19t408400367q6/xxlarge1089.gif) ![rcy](/content/qh19t408400367q6/xxlarge1088.gif) ![acy](/content/qh19t408400367q6/xxlarge1072.gif) ![vcy](/content/qh19t408400367q6/xxlarge1074.gif) ![ncy](/content/qh19t408400367q6/xxlarge1085.gif) ![ycy](/content/qh19t408400367q6/xxlarge1099.gif) 10–4 M.
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