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New studies of the plasma emission detector
Authors:Markus W Bradter  Wolfgang H Buscher  Karl Cammann  Michael J Faust  Frank G Winter
Institution:(1) Lehrstuhl für Analytische Chemie, Westfälische Wilhelms-Universität, Wilhelm-Klemm-Strasse 8, D-4400 Münster, Federal Republic of Germany
Abstract:Being an element-selective detector, the plasma emission detector was used to determine carbon in organic compounds. Experiments were carried out with the aid of osculating interference filters and lock-in amplifiers. The obtained signals were processed by a fast-Fourier-transform analyzer to study their frequency spectra. Results are given for the detection of carbon. Furthermore studies on the influence of angle-adjustment, microwave power, photomultiplier voltage and oscillation frequency on the determination of fluorine in organic compounds were carried out and results for detection limits and dynamic range of this method are presented.Presented in part at the 1989 European Winter Conference on Plasma Spectrochemistry, Reutte, Austria
Keywords:plasma emission detector  microwave-induced plasma  elementselective gas Chromatographic detector  fluorine determination  fast-Fourier-transform-analysis
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