Development and applications of sample controlled thermomicroscopy |
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| Authors: | Charsley E L Stewart C Barnes P A Parkes G M B |
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| Institution: | (1) Huddersfield University Queensgate, Hudersfield, HD1 3DH, UK;(2) Centre for Thermal Studies, University of Huddersfield Queensgate, Huddersfield, HD1 3DH, UK;(3) Centre for Applied Catalysis, School of Applied Sciences, University of Huddersfield Queensgate, Huddersfield, HD1 3DH, UK;(4) Centre for Applied Catalysis, University of Huddersfield Queensgate, Huddersfield, HD1 3DH, UK |
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| Abstract: | Sample controlled thermal analysis techniques such as constant rate transformation analysis or stepwise isothermal analysis,
where the transformation rate of the sample itself is used to control the experiment, are becoming increasingly important
1]. The measurements are normally carried out using changes in the sample mass, sample dimensions or in the evolved gas,
as the property used to control the experiment, and enable reactions to be studied in greater detail than is possible using
linear heating techniques. A new approach is described here where a thermomicroscopy system has been developed to enable the
intensity of the light reflected or transmitted by the sample to be used as the controlling signal 2].
This revised version was published online in July 2006 with corrections to the Cover Date. |
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