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Synthesis and structure of <Emphasis Type="Italic">N</Emphasis>-(2-(1-adamantyl)-2-hydroxyethyl)cytisine diastereomers |
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| Authors: | D V Shishkin E R Mukhamed’yarova N Z Baibulatova V A Dokichev Yu V Tomilov |
| Institution: | (1) Institute of Organic Chemistry, Ufa Scientific Center, Russian Academy of Sciences, Russia;(2) N. D. Zelinskii Institute of Organic Chemistry, Russian Academy of Sciences, Moscow |
| Abstract: | Diastereomers of N-(2-(1-adamantyl)-2-hydroxyethyl)cytisine were synthesized by reduction of N-(2-(1-adamantyl)-2-oxoethyl)cytisine with NaBH4. Their structures were established using x-ray structure analysis. __________ Translated from Khimiya Prirodnykh Soedinenii, No. 3, pp. 244–247, May–June, 2007. |
| Keywords: | synthesis cytisine derivatives diastereomers 15(R)- and 15(S)-N-(2-(1-adamantyl)-2-hydroxyethyl)cytisine x-ray structure analysis PMR 13C NMR |
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