The investigation of an equilibrium dependent reaction for the formation of enamines in a microchemical system |
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Authors: | Sands M Haswell S J Kelly S M Skelton V Morgan D O Styring P Warrington B |
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Affiliation: | Department of Chemistry, Faculty of Science and the Environment, University of Hull, Cottingham Road, Hull, UKHU6 7RX. |
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Abstract: | The paper describes the equilibrium dependant reaction for the formation of enamines in a microchemical system utilising electroosmotic flow (EOF) for fluid mobilisation. The authors have shown that the reaction can be carried out without the presence of a Lewis acid catalyst, in addition the enamine intermediate was synthesised at room temperature using mild solvent conditions. A 42% conversion of cyclohexanone into the enamine has been achieved to date. |
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