Measurement of orientation distributions using chemical shift amplification |
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| Authors: | Crockford Charles Geen Helen Titman Jeremy J |
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| Institution: | School of Physics and Astronomy, University of Nottingham, University Park, Nottingham, NG7 2RD, United Kingdom. |
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| Abstract: | A new three-dimensional magic angle spinning (MAS) experiment is proposed, based on a combination of the two-dimensional rotor-synchronized MAS experiment of Spiess and co-workers and a new chemical shift anisotropy amplification method. The new experiment is demonstrated on a macroscopically ordered sample of ultra-high molecular weight poly(ethylene). |
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