| 烯丙基乙基醚接枝聚硅氧烷气相色谱固定相的研究 |
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| 引用本文： | 高尧华,吴波,牛妍妍,周阳. 烯丙基乙基醚接枝聚硅氧烷气相色谱固定相的研究[J]. 分析测试技术与仪器, 2011, 17(2): 88-91 |
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| 作者姓名： | 高尧华 吴波 牛妍妍 周阳 |
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| 作者单位： | 山东大学化学与化工学院,山东济南,250100 |
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| 基金项目： | 山东省自然科学基金资助项目资助项目(No.2008ZRB01131) |
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| 摘 要： | 合成了侧链为烯丙基乙基醚的聚硅氧烷气相色谱固定相，静态法涂柱，评价了其色谱性能.该固定相柱效高，易于涂渍，耐温达290℃，分离选择性好，适用于醇类和酯类的分离以及白酒样品的分析.
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| 关 键 词： | 毛细管气相色谱 烯丙基乙基醚接枝聚硅氧烷 固定相 |
| 收稿时间： | 2011-05-17 |
| 修稿时间： | 2011-06-14 |
Allyl Ethyl Ether Polysiloxane as Stationary Phase for Capillary Gas Chromatography |
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| GAO Yao-hu,WU Bo,NIU Yan-yan and ZHOU Yang. Allyl Ethyl Ether Polysiloxane as Stationary Phase for Capillary Gas Chromatography[J]. Analysis and Testing Technology and Instruments, 2011, 17(2): 88-91 |
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| Authors: | GAO Yao-hu WU Bo NIU Yan-yan ZHOU Yang |
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| Affiliation: | GAO Yao-hua,WU Bo,NIU Yan-yan,ZHOU Yang(Department of Chemistry and Chemical Engineering,Shandong University,Jinan 250100,China) |
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| Abstract: | Polysiloxane with allyl ethyl ether as the side chain has been synthesized and used as stationary phase for capillary gas chromatography.The chromatography performance of these columns have been evaluated.The new stationary phase is proved to have high column efficiency and can easily coated using a static method,and its thermostability is up to 270 ℃,which is suitable for the separation of alcohols,esters and white spirit. |
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| Keywords: | capillary gas chromatography allyl ethyl ether polysiloxane stationary phase |
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