| 共沉淀法合成Cr3+∶Al2O3纳米粉体及其发光性能研究 |
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| 引用本文： | 米晓云,张希艳,卢 歆,柏朝晖,卢利平. 共沉淀法合成Cr3+∶Al2O3纳米粉体及其发光性能研究[J]. 无机化学学报, 2007, 23(10): 1819-1823 |
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| 作者姓名： | 米晓云 张希艳 卢 歆 柏朝晖 卢利平 |
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| 作者单位： | 长春理工大学材料科学与工程学院,长春,130022 |
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| 基金项目： | 长春理工大学校科研和教改项目 |
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| 摘 要： | NH4MO(OH)HCO3(M=Al3+， Cr3+) precursors were synthesized by a co-precipition method with the solutions of mixed nitrates as starting materials and ammonium bicarbonate as precipitator. The precursors and powders sintered at various temperatures were characterized by thermogravimetry/differential thermal analysis(TG/DTA)， infrared spectroscopy(IR)， X-ray diffractormetry(XRD)， transmittion electron microscopy(TEM). The luminescent spectra of Cr3+∶Al2O3 nano-powder was measured. The XRD results show that the pure-α-Al2O3 phase can be obtained at 1 200 ℃. TEM analysis indicates that the nano-powders about 20～30 nm are well-dispersed and less-aggregated. Spectral analysis demonstrates that the sample has good photoluminescence.
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| 关 键 词： | Cr3+:Al2O3 共沉淀法 纳米粉体 发光 |
| 文章编号： | 1001-4861（2007）10-1819-05 |
| 修稿时间： | 2007-06-20 |
Preparation and Luminescent Properties of Cr3+:Al2O3 Powders by Precipition Method |
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| MI Xiao-Yun,ZHANG Xi-Yan,LU Xin,BAI Zhao-Hui and LU Li-Ping. Preparation and Luminescent Properties of Cr3+:Al2O3 Powders by Precipition Method[J]. Chinese Journal of Inorganic Chemistry, 2007, 23(10): 1819-1823 |
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| Authors: | MI Xiao-Yun ZHANG Xi-Yan LU Xin BAI Zhao-Hui LU Li-Ping |
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| Affiliation: | School of Material Science and Engineering, Changchun University of Science and Technology, Changchun 130022 |
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| Abstract: | |
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| Keywords: | Cr3 :Al2O3 |
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