Thermal decomposition of [bis(salicylaldehydato)cadmium(II)] to CdS nanocrystals |
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| Authors: | Fatemeh Davar Masoud Salavati-Niasari Mehdi Mazaheri |
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| Institution: | 1. Institute of Nano Science and Nano Technology, University of Kashan, P.O. Box 87317-51167, Kashan, Islamic Republic of Iran;2. Department of Inorganic Chemistry, Faculty of Chemistry, University of Kashan, P.O. Box 87317-51167, Kashan, Islamic Republic of Iran;3. Materials and Energy Research Center, P.O. Box 14155-4777, Tehran, Islamic Republic of Iran |
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| Abstract: | The present investigation reports, the novel synthesis of nanocrystals CdS using thermal decomposition of bis(salicylaldehydato)cadmium(II)], as a new precursor, and elemental sulfur in oleylamine. The as-synthesized CdS crystals have diameters about 10 nm. The products were characterized by X-ray diffraction (XRD) transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), ultraviolet–visible (UV–Vis) spectroscopy and Fourier transformed infrared (FT-IR) spectra. The results of this paper show that the shape and size of cadmium sulfide nanocrystals can be controlled systematically by adjusting certain reaction parameters, such as the reactant concentration, the reaction temperature and the reaction time. Cadmium sulfide nanoparticles and nanorods with different lengths have been successfully prepared. |
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