Crystal and molecular structure ofN,N′,N″-tritosyl-5,8,14,17,23,26-hexamethyl-2,11,20-triaza[3.3.3]-paracyclophane 1 : 1 dichloromethane clathrate期刊界 All Journals 搜尽天下杂志传播学术成果专业期刊搜索期刊信息化学术搜索

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Crystal and molecular structure ofN,N′,N″-tritosyl-5,8,14,17,23,26-hexamethyl-2,11,20-triaza[3.3.3]-paracyclophane 1 : 1 dichloromethane clathrate

Authors:	F Bottino P Finocchiaro J Lipkowski A Mamo S Pappalardo K Suwinska

Institution:	(1) Dipartimento di Scienze Chimiche, Universita' di Catania, Viale A. Doria 8, 95125 Catania, Italy;(2) Istituto Chimico, Facolta' di Ingegneria, Universita' di Catania, Viale A. Doria 6, 95125 Catania, Italy;(3) Institute of Physical Chemistry, Polish Academy of Sciences, Kasprzaka 44/52, 01-224 Warsaw, Poland

Abstract:	The crystal and molecular structure of the title compound, C₅₁H₅₇N₃O₆S₃·CH₂Cl₂ has been determined by single crystal X-ray analysis and refined to anR-value of 0.069 for 1032 reflections. The crystal is trigonal, space groupR3, witha = 21.255(7),c = 11.317(4), andZ = 3. One molecule of dichloromethane used as solvent is enclathrated in the crystal lattice.

Keywords:	N-tosyl azamacrocycles crystal structure clathrate formation
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