Influence of pressure reduction on the shapes of thermoanalytical curves of red muds |
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Authors: | K Papp É Kocsárdy A Kiss T Lakatos |
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Institution: | (1) ALUTERV-FKI, Budapest;(2) Tungsram, Budapest, Hungary |
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Abstract: | The effect of reduction of pressure on the shapes of the TG, DTG and DTA curves and the mass-spectra of hydroxide and carbonate phases was investigated in some typical Hungarian red muds. The pressure change caused different decomposition rates of the phases and resulted in better separation of the overlapping thermal curves; this led to advantages as regards phase analysis. For phase analysis the red muds were extracted with water, and the extracts and solid residues were identified by IR- and X-ray methods.
Zusammenfassung Die Wirkung der Druckänderung auf die Form der TG-, DTG- und DTA-Kurven, sowie der MS-Spektra der Hydroxid- und Carbonatphasen in einigen typischen ungarischen Rotschlamm-Sorten wurde geprüft. Die Druckänderung verursachte verschiedene Zersetzungsgeschwindigkeiten der Phasen, führte zur besseren Auftrennung der sich überlappenden thermischen Kurven, und war ausserdem auch hinsichtlich der Phasenanalyse vom Vorteil. Zur Phasenanalyse wurden die Rotschlämme mit Wasser extrahiert und die Extrakte und festen Rückstände mittels IR- und Röntgenmethoden identifiziert.
Résumé On a étudié dans quelques espèces typiques de boues rouges de Hongrie l'effet des variations de pression sur la forme des courbes TG, TGD et ATD ainsi que les spectres de masse des phases hydroxyde et carbonate. La variation de la pression entraîne des vitesses de décomposition différentes. Il en résulte une meilleure séparation des phénomènes dans le cas où ceux-ci se chevauchent ainsi que des avantages du point de vue de l'analyse des phases. L'analyse des phases présentes dans les boues rouges a été effectuée par extraction à l'eau. Les extraits et les résidus solides ont été identifiés par spectrométrie infrarouge et par diffraction des rayons X.
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![acy](/content/u2j42l51773654v8/xxlarge1072.gif) ![scy](/content/u2j42l51773654v8/xxlarge1089.gif) ![ncy](/content/u2j42l51773654v8/xxlarge1085.gif) ![ocy](/content/u2j42l51773654v8/xxlarge1086.gif) ![scy](/content/u2j42l51773654v8/xxlarge1089.gif) ![pcy](/content/u2j42l51773654v8/xxlarge1087.gif) ![iecy](/content/u2j42l51773654v8/xxlarge1077.gif) ![kcy](/content/u2j42l51773654v8/xxlarge1082.gif) ![tcy](/content/u2j42l51773654v8/xxlarge1090.gif) ![ocy](/content/u2j42l51773654v8/xxlarge1086.gif) ![scy](/content/u2j42l51773654v8/xxlarge1089.gif) ![kcy](/content/u2j42l51773654v8/xxlarge1082.gif) ![ocy](/content/u2j42l51773654v8/xxlarge1086.gif) ![pcy](/content/u2j42l51773654v8/xxlarge1087.gif) ![icy](/content/u2j42l51773654v8/xxlarge1080.gif) ![iecy](/content/u2j42l51773654v8/xxlarge1077.gif) .
Paper presented at the Scientific Session on Thermal Analysis held at Balatonfüred, Hungary, on 14–16 October 1976. |
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