The crystal structure of 2-benzoylpyridine N4-methyl-N4-phenylthiosemicarbazone |
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| Authors: | Jesús Valdés-Martínez Simon Hernández-Ortega Douglas X. West Amy M. Stark Gordon A. Bain |
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| Affiliation: | (1) Instituto de Química, Universidad Nacional Autónoma de México, Circuito Exterior, Ciudad Universitaria, Coyoacán, 04510 México, D.F.;(2) Department of Chemistry, Illinois State University, 61790-4160 Normal, Illinois |
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| Abstract: | 2-Benzoylpyridine N4-methyl-N4-phenylthiosemicarbazone, HBz4MePh, monoclinic,P2(1)/n a=9.141(2),b=18.507(4),c=11.401(2) Å,  =110.58(3)o,V=1805.6(9) Å3,Z=4,  =1.655 mm–1. HBz4MePh crystallizes in a hydrogen bonded Z isomeric conformation with respect to the C7–N2 bond. The intramolecular hydrogen bond is between N3–H...N1, and the S atom isZ to the azomethine nitrogne, N2. |
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| Keywords: | Thiosemicarbazone 2-benzoylpyridine N4-substituted hydrogen bonding |
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