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Synthesis and Vibrational Studies of Oxovanadium (IV) - Tetradentate Schiff Base Complexes
Authors:S M Teleb  S A Sadeek  E M Nour
Institution:Department of Chemistry, Faculty of Science , Zagazig University , Zagazig, Egypt
Abstract:The two new Schiff base complexes of oxovanadium (IV) VO(acac-en)] (acac-en = bisacetylactone-ethylenediimino) and VO(sal-o-phdn)] (sal-o-phdn = N,N′-o-phenylenebis (salicylideneiminato) have been prepared. The infrared spectra of the solid complexes have been obtained and assigned on the bases of Cs symmetry. A polymeric chain structure with V-O-V bridge has been adopted for the both complexes.
Keywords:Two-dimensional NMR  homonuclear chemical shift correlation  acetophenone glycoside  solanaceous cells
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