Thermal Degradation of Polysiloxane Coatings on E-Glass Fiber. A FTIR Study |
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Authors: | A. Larena M. C. Matías J. Martínez Urreaga |
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Affiliation: | Dpto. Ing. Química Ind., E.T.S.I. Industriales , U. Politécnica de Madrid , 28006, Madrid |
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Abstract: | Fourier Transform Infrared Spectroscopy and Thermal Analysis have been used to study the thermal and termooxidative degradation of polysiloxane coatings obtained by treating E-glass fiber with aqueous solutions of 3-chloropropyltriethoxysilane. Initial weight losses were due to polymerization of the coatings. Severe oxidative degradations were observed at temperatures above 180°C. At 550°C the residue of the coating was found to be silica with free silanol groups. |
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Keywords: | FTIR Spectroscopy E-Glass Fiber Polysiloxane Coatings Thermal Degradation |
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