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Thermal Degradation of Polysiloxane Coatings on E-Glass Fiber. A FTIR Study
Authors:A Larena  M C Matías  J Martínez Urreaga
Institution:Dpto. Ing. Química Ind., E.T.S.I. Industriales , U. Politécnica de Madrid , 28006, Madrid
Abstract:Fourier Transform Infrared Spectroscopy and Thermal Analysis have been used to study the thermal and termooxidative degradation of polysiloxane coatings obtained by treating E-glass fiber with aqueous solutions of 3-chloropropyltriethoxysilane. Initial weight losses were due to polymerization of the coatings. Severe oxidative degradations were observed at temperatures above 180°C. At 550°C the residue of the coating was found to be silica with free silanol groups.
Keywords:FTIR Spectroscopy  E-Glass Fiber  Polysiloxane Coatings  Thermal Degradation
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