Synthesis of 2,2,6,6-tetramethyl-1-oxyl-4-piperidyloxy-tert-butylperoxyalkylsilanes期刊界 All Journals 搜尽天下杂志传播学术成果专业期刊搜索期刊信息化学术搜索

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Synthesis of 2,2,6,6-tetramethyl-1-oxyl-4-piperidyloxy-tert-butylperoxyalkylsilanes

Authors:	E A Gruzinova A K Litkovetz E V Gruzinov

Institution:	(1) Institute of Synthetic Polymeric Materials, Russian Academy of Sciences, 70 ul. Profsoyuznaya, 117393 Moscow, Russian Federation

Abstract:	2,2,6,6-Tetramethyl-1-oxyl-4-piperidyloxy-tert-butylperoxyalkylsilanes were obtained by condensation of 2,2,6,6-tetramethyl-4-hydroxypiperidine-1-oxyl with organosilicon chloroperoxides ClR₂SiOOR' (R = Me, Et; R' = Bu^t) in ether at 0–5 °C in the presence of a tertiary amine as an HCl acceptor.Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 5, pp. 984–985, May, 1995.

Keywords:	2 2 6 6-tetramethyl-4-hydroxypiperidine-1-oxyl organosilicon chloroperoxides condensation 2 2 6 6-tetramethyl-1-oxyl-4-piperidyloxy-tert-butylperoxyalkylsilanes
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