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火焰原子吸收法测定中药土大黄中四种微量元素的含量
引用本文:罗人仕,胡馨,廖建华.火焰原子吸收法测定中药土大黄中四种微量元素的含量[J].广东微量元素科学,2014,0(8):15-18.
作者姓名:罗人仕  胡馨  廖建华
作者单位:罗人仕 (赣南医学院药学院,江西 赣州,341000); 胡馨 (赣南医学院药学院,江西 赣州,341000); 廖建华 (赣南医学院药学院,江西 赣州,341000);
基金项目:江西省卫生厅中医药科研计划课题(项目编号:2013A043)赣南医学院课题(项目编号:YB201319,,QD201303)
摘    要:目的运用火焰原子吸收光谱法测定中药土大黄根中的Fe、Zn、Mg、Ca等4种金属元素的含量。方法用浓HNO3-HClO4消解样品,采用标准曲线法测定其4种金属元素含量。结果所测的样品中含有丰富的人体必需微量元素,尤其是Ca含量极高。方法回收率在96.90%~102.3%之间,样品相对偏差小于5%。结论方法简单、准确,结果令人满意。

关 键 词:火焰原子吸收光谱法  土大黄  微量金属元素

Determination of Four Trace Elements in Rumex Nepalensis by FAAS
LUO Renshi,HU Xin,LIAO Jianhua.Determination of Four Trace Elements in Rumex Nepalensis by FAAS[J].Trace Elements Science,2014,0(8):15-18.
Authors:LUO Renshi  HU Xin  LIAO Jianhua
Institution:( Department of Pharmacy, Gannan Medical University, Jiangxi Ganzhou 341000, China)
Abstract:Objective The contents of Fe, Zn, Mg and Ca in rumex nepalensis were analyzed by flame atomic absorption spectrometry. Methods The sample was pretreated with HNO3 - HClO4 and measured quantitatively through calibration curve method. Results It was shown that the sample has rich in human essential metal elements. The recoveries are between 96. 90 % and 102. 3 %, and the relative standard deviation is less than 5%. Conclusion The result measured by this method is considered to be accurate.
Keywords:FAAS  rumex nepalensis  rare metal elements
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