Synthesis and characterization of 5-bromo-3-sec-butyl-6-methyluracil |
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| Authors: | Huixue Ren Yanzhao Yang Jimao Lin Yinshan Qi Yeqing Zhang |
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| Affiliation: | (1) School of Environmental Engineering, Shangdong Jianzhu University, Jinan, 250010, China;(2) School of Chemistry and Chemical Engineering, Shandong University, Jinan, 250001, China;(3) ZiBo HuaLian Mining Industry CO., LTD, Zibo, 256100, China |
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| Abstract: | A new synthetic method for 5-bromo-3-sec-butyl-6-methyluracil (Bromacil) using 2-bromobutane and urea as starting materials is described. The synthesis involved condensation, cyclization and bromination with a total yield of 60%. The structure of Bromacil was determined by 1H NMR, 13C NMR and IR spectroscopy. __________ Translated from Journal of Shandong University (Natural Science Edition), 2007, 42(7): 9–12 [译自: 山东大学学报(自然科学版)] |
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| Keywords: | Bromacil condensation cyclization bromination |
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