| 中空型的Ag/Pd和Ag/Pt纳米立方的一锅合成及其光学性能表征 |
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| 引用本文： | 吴绒,胡冠琦,胡建强. 中空型的Ag/Pd和Ag/Pt纳米立方的一锅合成及其光学性能表征[J]. 光散射学报, 2012, 24(3): 316-320 |
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| 作者姓名： | 吴绒 胡冠琦 胡建强 |
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| 作者单位： | 1. 华南理工大学化学与化工学院化学系,广州,510640
2. 华南理工大学化学与化工学院化学系,广州510640;华南理工大学化学与化工学院 制浆造纸国家重点实验室,广州510640 |
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| 基金项目： | 国家自然科学基金面上项目(21173087);华南理工大学中央高校基本科研业务费(SCUT2009ZZ0010);制浆造纸国家重点实验室开放基金项目(200904) |
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| 摘 要： | 本文通过改进的多元醇法成功制备了尺寸可控、均一的立方形银纳米材料, 然后在不经过任何后处理的情况下通过置换反应一锅合成了中空型的银/钯(Ag/Pd)和银/铂(Ag/Pt)纳米立方体, 并用透射电子显微镜(TEM)和紫外可见吸收(UV-visible)光谱对所合成的Ag纳米立方和空心的Ag/Pd 和Ag/Pt纳米立方进行了表征。
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| 关 键 词： | 银/钯(Ag/Pd) 银/铂(Ag/Pt) 纳米立方体 中空结构 一锅合成 表征 |
| 收稿时间： | 2011-06-30 |
One-pot Synthesisand Spectroscopic Characterization of Hollow Ag/Pd and Ag/Pt Nanocubes |
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| WU Rong , HU Guan-qi , HU Jian-qiang. One-pot Synthesisand Spectroscopic Characterization of Hollow Ag/Pd and Ag/Pt Nanocubes[J]. Chinese Journal of Light Scattering, 2012, 24(3): 316-320 |
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| Authors: | WU Rong HU Guan-qi HU Jian-qiang |
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| Affiliation: | 1,2(1.Department of Analytical Chemistry,College of Chemistry and Chemical Engineering, South China University of Technology,Guangzhou 510640,China; 2.State Key Laboratory of Pulp and Paper Engineering,South China University of Technology,Guangzhou 510640,China) |
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| Abstract: | Hollow silver/palladium(Ag/Pd) and silver/platinum(Ag/Pt) nanocubes were fabricated for the first time through one-pot galvanic replacement method using Pd or Pt precursors and the template of freshly prepared Ag nanocubes,in which silver nanocubes were synthesized by a modified polyol reduction method.The compositions,sizes,and shapes of the Ag and hollow Ag/Pd and Ag/Pt nanocubes were characterized by transmission electron microscopy(TEM) and ultraviolet-visible(UV-visible) spectroscopy. |
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| Keywords: | silver/palladium(Ag/Pd) silver/platinum(Ag/Pt) hollow structure nanocube one-pot synthesis characterization |
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